Amity Journal of Behavioural and Forensic Sciences

  • Year: 2008
  • Volume: 4
  • Issue: 1

Detection and Characterization of Kerosene in Fire Debris by Thin Layer Chromatography

  • Author:
  • A. K. Jaiswal1, T. Millo1, G. K. Gaur2, R. C. Sharma3, N. Lal4, S. K. Mewar5, N. G. Giri6
  • Total Page Count: 4
  • DOI:
  • Page Number: 593 to 596

1Dept. of Forensic Medicine and Toxicology, All India Institute of Medical Sciences, New Delhi-110029.

2Regional Forensic Science Laboratory, City Centre, Gwalior - 474002, M.P.

3State Forensic Science Laboratory, Nehru Nagar, Jaipur, Rajasthan-302003.

4Dept. of Chemistry, V.S.S.D. College, Kanpur - 208002, U.P.

5Dept. of NMR, All India Institute of Medical Sciences, New Delhi-110029.

6Dept. of Chemistry, Delhi University, Delhi - 110007.

Abstract

A sensitive and selective thin layer chromatographic method for the detection of kerosene in fire debris using chloranil as a spray reagent has been developed. In this method, ether extract of partially burnt clothes encountered in homicidal, suicidal burning/fire and arson was separated for its different constituents by T.L.C. using new developing solvent system Heptane: Acetone (6:4) and spraying reagent Chloranil followed by H2SO4 which was confirmed with fresh Kerosene, Kerosene residue, Napthalene, 2-Methyl napthalene and 2,6-Dimethyl naphthalene. This method is fast, easy, inexpensive, sensitive and selective for the detection and characterization of kerosene and its residues in forensic Laboratory.

Keywords

TLC, Kerosene, Chloranil, Kerosene residue, Naphthalene, 2-Methyl Naphthalene, 2,6-Dimethyl Naphthalene etc