Asian Journal of Research In Chemistry
  • Year: 2012
  • Volume: 5
  • Issue: 10

Synthesis and Spectroscopic Studies of Mixed 2-(N-Salicylidene)-5- Chlorobenzophenone Dialkyldithiophosphato Derivatives of Antimony(III)

  • Author:
  • K. Prasada Rao1,, M. S. Singh2, K. Santhakumari1
  • Total Page Count: 4
  • Page Number: 1225 to 1228

1Dept. of Chemistry, Bapatla Engineering College, Bapatla (Autonomous)-522101, Andhra Pradesh, India

2Professor, Banarus Hindu University, Varanasi, (U.P.) India

*Corresponding Author E-mail: prasad17467@gmail.com

Online published on 7 February, 2013.

Abstract

Some Antimony(III) derivatives of schiff base derived from 2-(N-salicylidene)-5-chlorobenzophenone have been synthesized by the reaction of dichloro and chlorobis 2-(N-salicylidene)-5-chlorobenzophenone antimony(III) with ammonium dialkyldithiophosphates in benzene (prepared insitu) in 1:2 and 1:1 molar ratios, respectively. All these compounds are characterized by elemental analysis, molecular weight measurements and spectroscopic (IR, 1H and 31P NMR) studies.

Keywords

Schiff base ligands, alkyldithiocarbonate, dialkyldithiophosphato