Asian Journal of Research In Chemistry
  • Year: 2014
  • Volume: 7
  • Issue: 8

Synthesis, Characterization and Study of Chromatography Behavior of Novel (Azo–Anil)-Heterocyclic Compounds

  • Author:
  • Nagham Mahmood Aljamali1,, Khdeeja Jabbar Ali1, Nuha Salman Salih2, Sajida Hadi Ridha1
  • Total Page Count: 9
  • Page Number: 702 to 710

1Assist. Professor, Dept. of Chem., Educt. College, Kufa Univ., Iraq

2Lecturer, Dept of Chem., Science College, Kufa Univ., Iraq

*Corresponding Author E-mail: dr.Nagham_mj@yahoo.com

Online published on 22 October, 2014.

Abstract

The present work included synthesis of novel (azo-anil) compounds in high yield, which react with (chloro acetyl chloride, sodium azide, alanine, o-thiol via condensation reaction to produce various heterocycles (four, five, six, seven) membered ring like (azetidine, imidazole, thiazine, oxazepine, diazepine, tetrazole) The structure of the newly synthesized compounds were monitored by (TLC) and identified by many techniques (FT.IR, 1H.NMR, C.H.N), melting points and study of chromatography behavior.

Keywords

Chromatography, azo–anil, heterocycle, thiazine, diazepine