College of Chemistry and Chemical Engineering, Central South University, ChangSha, Hunan, 410083, PR China.
Syn-2-furyl-2-(methoxyimino) acetic acid was prepared from 2-acetyl-furan after oximation, hydrolysis, oxidation, and then condensation with methoxylamine hydrochloride, the total yield was 37.8%. The suitable experimental conditions were also discussed.
syn-2-furyl-2-(methoxyimino) acetic acid, 2-acetyl-furan, methoxylamine hydrochloride, hydrolysis, oximation, condensation