Indian Journal of Entomology
Open Access
SCOPUSWeb of Science
  • Year: 2021
  • Volume: 83
  • Issue: 4

Residues of Thiamethoxam 12.6%+ Lambda Cyhalothrin 9.5%ZC in Vegetable Cowpea

1Department of Agricultural Entomology, Kerala Agricultural University, Thiruvananthapuram695522, Kerala, India

Department of Agricultural Entomology, Tamil Nadu Agricultural University, Coimbatore641003, Tamil Nadu, India

*Email: bankakishorereddy@gmail.com (corresponding author)

Abstract

A field experiment was conducted to study the rate of dissipation of insecticide mixture (thiamethoxam 12.6%+ lambda cyhalothrin 9.5%ZC) in vegetable cowpea. The insecticide mixture @ 0.30 ml l-1 was sprayed at pod formation stage, and samples of pods were harvested at 0 (2 hr after spray), and 1, 3, 5, 7, 10, 15 days after spray. The residues were estimated using liquid chromatography tandem mass spectrometer (LC MS/ MS) and GC-ECD at the All India Network Project on Pesticides Residues, College of Agriculture, Vellayani, Kerala. The residues of thiamethoxam and lambda cyhalothrin were found to be 0.12 and 0.21 µg g-1, respectively. Residues were observed to persist up to three days, and were below detectable level on the fifth day.

Keywords

Lambda cyhalothrin, Thiamethoxam, Vegetable cowpea, Dissipation, Residue, Risk assessment, Food safety, LCMS, GC-ECD, Method validation, Recovery, Linearity