International Journal of Meterials Sciences

  • Year: 2009
  • Volume: 4
  • Issue: 2

Low-Temperature Synthesis of ZnO by Wet Chemical Method

  • Author:
  • Ashkan Keshavarzi1, Abdul Halim Abdullah1,2, Zulkarnain Zainal1,2
  • Total Page Count: 6
  • DOI:
  • Page Number: 163 to 168

1Department of Chemistry, Faculty of Science, Universiti Putra Malaysia, 43400, Serdang, Selangor D.E., Malaysia.

2Advanced Materials and Nanotechnology Laboratory, Advanced Institute of Technology, Universiti Putra Malaysia, 43400, Serdang, Selangor D.E., Malaysia.

Abstract

Zinc oxide (ZnO) wire was synthesized by hydrothermal method at 70° C by using Zn acetate dihydrate and ammonium hydroxide as the starting material. The sample was characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), electron disperse X-ray (EDX), electro diffraction (ED) and transmission electron microscopy (TEM). The XRD result confirmed the formation of ZnO with wurtzite structure. The ED reveals that ZnO wire is single crystal and grows up along [001] direction. Influence of temperature on crystal growth was evaluated. Results shown that increase in temperature shorten the length of wire.

Keywords

ZnO, hydrothermal, crystal growth