Journal of Metallurgy and Materials Science
  • Year: 2010
  • Volume: 52
  • Issue: 2

Preparation and characterization of polyaniline-NiO nanocomposites via interfacial polymerization

  • Author:
  • Mahesh D. Bedre, S. Basavaraja1, Raghunandan Deshpande2, Balaji D. Sawle1, Arun Kumar Lagashetty3, B. Govindraj4, A. Venkataraman
  • Total Page Count: 6
  • Page Number: 149 to 154

1Veeco-India Nanotechnology Laboratory, Jawaharalal Nehru Centre for Advanced Scientific Research, Bangalore, Karnataka, India.

2H.K.E College of Pharmacy, Sedam Road, Gulbarga, Karnataka, India.

3Appa Institute of Engineering and Technology, Gulbarga, Karnataka, India.

4Vijayanagara Degree College Hospet, Karnataka, India.

Materials Chemistry Laboratory, Gulbarga University, Gulbarga-585106, Karnataka, India.

* Corresponding Author Email: raman_chem@rediffmail.com

Abstract

Polyaniline-NiO nanocomposites were prepared by employing interfacial polymerization using ammonium persulphate as an oxidizing agent. The formations of regular nanocomposite materials were studied by Fourier transform infrared (FTIR) spectroscopy and XRD techniques. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) images were conducted to characterize the morphology. Thermo gravimetric (TG) analysis was carried out study the thermal stability of the resulting composites. Formation of conducting emeraldine salt form was concluded by electrical conductivity.

Keywords

Interfacial polymerization, Polyaniline, NiO nanocomposites, conductivity